15-20 November 2015
Virtual
Africa/Johannesburg timezone
The 1st African Light Source Conference and Workshop

The Use of Diffraction to Determine the Residual Stress of HVOF WC-17Co Coatings

17 Nov 2015, 17:20
20m
Auditorium (ESRF)

Auditorium

ESRF

71 avenue des Martyrs, 38000 Grenoble, France
Oral Presentations Main Scientific Talks

Speaker

Dr O.P. Oladijo ((1) Department of Chemical, Materials and Metallurgical Engineering, Botswana International University of Science and Technology, Palapye, Botswana (2) School of Chemical and Metallurgical Engineering, University of the Witwatersrand, South Africa (3) DST/NRF Centre of Excellence in Strong Materials, University of the Witwatersrand South Africa)

Description

The investigation was conducted to determine the residual stresses of thermally sprayed HVOF WC-17Co coatings on different alloy substrates by non-destructive techniques. Non-destructive determination of residual stresses in the WC-Co coated systems was exceptionally challenging because coatings were only about 200 microns thick. The best-suited techniques for investigation of the WC coatings were diffraction-based strain scanning, using penetrating radiation such as thermal neutrons (most penetrating), high energy synchrotron X-rays (100 keV enables 20 micron penetration) and laboratory X-rays (limited to 5 micron penetration). Laboratory X-rays (Necsa, using Co radiation), thermal neutrons (ANSTO, Australia) and X-ray synchrotron (ESRF, France) were successfully employed to resolve the stress conditions. The influence of heat treatment was assessed by understated stress relief heat treatment of the grit-blasted substrates and coated substrates. The surface stresses of the coatings exhibited both small compressive and low tensile stresses on the as-sprayed coated samples. After annealing, the stresses became substantially more compressive. The near-surface trends of the grit-blasted substrates were completely relaxed after annealing, with thermal stresses being the dominant mechanism for residual stress induced due to the large difference in the coefficients of thermal expansion (CTE) between the WC coatings and the substrates. References: [1] O.P. Oladijo, A.M. Venter, L.A. Cornish and N. Sacks, Surface Coating Technology, 206 (2012) 4725-4729 [2] A.M. Venter, T. Pirlin, T. Buslap, O.P. Oladijo, A. Steuwer, T.P. Ntsoane, L.A. Cornish and N. Sacks, Surface Coating Technology, 206 (2012) 4011-4020. [3] O.P. Oladijo, N. Sacks, L.A. Cornish and A.M. Venter, Int. J. of Refractory Metals and Hard Materials, 35 (2012) 288-294 [4] A.M. Venter, O.P. Oladijo, V. Luzin, L.A. Cornish and N. Sacks, Solid Films, 549 (2013) 330-339

Primary author

Dr O.P. Oladijo ((1) Department of Chemical, Materials and Metallurgical Engineering, Botswana International University of Science and Technology, Palapye, Botswana (2) School of Chemical and Metallurgical Engineering, University of the Witwatersrand, South Africa (3) DST/NRF Centre of Excellence in Strong Materials, University of the Witwatersrand South Africa)

Co-authors

Dr A.M. Venter ((1) Research & Development Division, NECSA Limited, Pretoria, South Africa (2) DST/NRF Centre of Excellence in Strong Materials, University of the Witwatersrand South Africa) Prof. L.A. Cornish ((1) School of Chemical and Metallurgical Engineering, University of the Witwatersrand, South Africa (2) DST/NRF Centre of Excellence in Strong Materials, University of the Witwatersrand South Africa) Prof. N. Sacks ((1) School of Chemical and Metallurgical Engineering, University of the Witwatersrand, South Africa (2) DST/NRF Centre of Excellence in Strong Materials, University of the Witwatersrand South Africa) Mr T.P. Ntsoane ((1) Research & Development Division, NECSA Limited, Pretoria, South Africa (2) DST/NRF Centre of Excellence in Strong Materials, University of the Witwatersrand South Africa)

Presentation Materials