7-11 July 2014
Africa/Johannesburg timezone
<a href="http://events.saip.org.za/internalPage.py?pageId=16&confId=34"><font color=#0000ff>SAIP2014 Proceedings published on 17 April 2015</font></a>

Microwave synthesis of graphene nickel aluminum layered double hydroxide (LDH)

8 Jul 2014, 17:10
1h 50m
D Ring ground level

D Ring ground level

Board: F.407
Poster Presentation Track F - Applied Physics Poster1

Speaker

Ms Fatemeh Taghizadeh (University of Pretoria)

Main supervisor (name and email)<br>and his / her institution

N.Manyala
Department of Physics SARCHI chair in carbon Technology University of Pretoria
Ncholu.manyala@up.ac.za

Level for award<br>&nbsp;(Hons, MSc, <br> &nbsp; PhD)?

MSc

Apply to be<br> considered for a student <br> &nbsp; award (Yes / No)?

yes

Would you like to <br> submit a short paper <br> for the Conference <br> Proceedings (Yes / No)?

no

Abstract content <br> &nbsp; (Max 300 words)<br><a href="http://events.saip.org.za/getFile.py/access?resId=0&materialId=0&confId=34" target="_blank">Formatting &<br>Special chars</a>

Layered double hydroxide (LDH) with petal-like platelets structure has been produced via microwave irradiation reaction within 1-3 hours by hydrolysis of urea with homogeneous solution of Nickel nitrate and Aluminum nitrate. The feed ratio of the Ni and Al, microwave reaction power and time has been optimized. Pure crystalline Layered double hydroxide (LDH) structure was obtained for feed ratio of 2.0 and reaction power of 100 W with growth time of 1 hour. The structure obtained shows uniform and homogeneous size distribution with high crystallinity. The sample was functionalized with graphene foam and the samples were characterized by x-ray diffraction (XRD), scanning electron microscope (SEM) and Raman spectroscope. The obtained LDH/graphene composite materials were tested as electrode for electrochemical capacitors and it demonstrate good capacitance behavior as potential candidate for energy storage applications.

Primary author

Ms Fatemeh Taghizadeh (University of Pretoria)

Co-authors

Mr Abdulhakeem Bello (University of Pretoria) Mr Damilola Momodu (University of Pretoria) Mr Farshad Barzegar (University of Pretoria) Mr Kadiou Dangbegnon (University of Pretoria) Dr Ncholu Manyala (University of Pretoria)

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